- Synthesis of Platinum Nanoparticles by Liquid Phase Reduction
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Jin-Ho Lee, Se-Hoon Kim, Jin-Woo Kim, Min-Ha Lee, Young-Do Kim
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J Korean Powder Metall Inst. 2012;19(1):60-66.
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DOI: https://doi.org/10.4150/KPMI.2012.19.1.060
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- In this study, Platinum(Pt) nanoparticles were synthesized by using polyol process which is one of the liquid phase reduction methods. Dihydrogen hexachloroplatinate (IV) hexahydrate (H_2PtCl_6cdot6H_2O), as a precursor, was dissolved in ethylene glycol and silver nitrate (AgNO_3) was added as metal salt for shape control of Pt particle. Also, polyvinylpyrrolidone (PVP), as capping agent, was added to reduce the size of particle and to separate the particles. The size of Pt nanoparticles was evaluated particle size analyzer (PSA). The size and morphology of Pt nanoparticles were observed by transmission electron microscopy (TEM) and high resolution TEM (HRTEM). Synthesized Pt nanoparticles were studied with varying time and temperature of polyol process. Pt nanoparticles have been successfully synthesized with controlled sizes in the range 5-10 and 20-40 nm with cube and multiple-cube shapes.
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Citations
Citations to this article as recorded by  - Facile Strategy for Mass Production of Pt Catalysts for Polymer Electrolyte Membrane Fuel Cells Using Low-Energy Electron Beam
Jongmin Shin, Jiho Min, Youngjin Kim, Jin Hee Lee, Geunseok Chai, Namgee Jung
Nanomaterials.2020; 10(11): 2216. CrossRef - Synthesis of Nanosized Nickel Particle from Spent Cathodic Material Containing Lithium
Jei-Pil Wang
Journal of Korean Powder Metallurgy Institute.2019; 26(4): 340. CrossRef - Fabrication and Characterization of Ag Particles by Polyol Process and Wet Chemical Process
Juyeon Yoo, Hyosung Jang, Kun-Jae Lee
Journal of Korean Powder Metallurgy Institute.2016; 23(4): 297. CrossRef
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